methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

Base Information

• Chemical Name: methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate
• CAS No.: 1149669-82-8
• Molecular Formula: C₃₈H₅₀Br₂N₄O₉
• Molecular Weight: 866.644

Synonyms:methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

Chemical Property of methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

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Technology Process of methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

There total 1 articles about methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid (1149669-99-7) + C17H23BrN2O4*ClH → methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate (1149669-82-8)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo900222g

Reference yield: 100.0%

methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate (1149669-82-8) → C33H42Br2N4O7*ClH (1149670-05-2)

Guidance literature:

With hydrogenchloride; In diethyl ether; dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo900222g

upstream raw materials:

(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

Downstream raw materials:

C₃₃H₄₂Br₂N₄O₇*ClH

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