(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

Base Information

Chemical Name:(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid
CAS No.:1149669-99-7
Molecular Formula:C₂₁H₂₉BrN₂O₆
Molecular Weight:485.375
Hs Code.:

Synonyms:(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

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Chemical Property of (S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

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Technology Process of (S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

There total 1 articles about (S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1149669-81-7
methyl (2S)-2-(2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

: 1149669-99-7
(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

Guidance literature:: With lithium hydroxide; water; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo900222g

Reference yield: 67.0%

: 1149669-99-7
(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

: C₁₇H₂₃BrN₂O₄*ClH

: 1149669-82-8
methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanamido)tetrahydrofuran-3-carboxamido)-3-methylbutanoate

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo900222g

Reference yield: 66.0%

: 1149669-99-7
(S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)tetrahydrofuran-3-carboxamido)-3-methylbutanoic acid

: 1149670-05-2
C₃₃H₄₂Br₂N₄O₇*ClH

: 1149669-83-9
methyl (S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-((S)-2-((2S,3R)-2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)-tetrahydrofuran-3-carboxamido)-3-methylbutanamido)-tetrahydrofuran-3-carboxamido)-3-methylbutanamido)-tetrahydrofuran-3-carboxamido)-3-methylbutanoate

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo900222g