N-(2,3-dimethylphenyl)benzenesulfonamide

Base Information

Chemical Name:N-(2,3-dimethylphenyl)benzenesulfonamide
CAS No.:126494-77-7
Molecular Formula:C₁₄H₁₅NO₂S
Molecular Weight:261.345
Hs Code.:
European Community (EC) Number:667-851-3
NSC Number:164384
Mol file:126494-77-7.mol

Synonyms:N-(2,3-dimethylphenyl)benzenesulfonamide;126494-77-7;NSC164384;Oprea1_486304;MFCD00091026;STL253670;AKOS000384611;NSC-164384;AN-652/41300208

Suppliers and Price of N-(2,3-dimethylphenyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-(2,3-dimethylphenyl)benzenesulfonamide

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:261.08234989
Heavy Atom Count:18
Complexity:355

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)NS(=O)(=O)C2=CC=CC=C2)C

Technology Process of N-(2,3-dimethylphenyl)benzenesulfonamide

There total 5 articles about N-(2,3-dimethylphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98-09-9
benzenesulfonyl chloride

: 87-59-2
2,3-Dimethylaniline

: 126494-77-7
2,3-dimethyl-N-(phenylsulfonyl)aniline

Guidance literature:: With pyridine; In dichloromethane;
DOI:10.1002/1099-0690(200207)2002:13<2094::AID-EJOC2094>3.0.CO;2-E

Reference yield:

: 476170-47-5
2-methoxycarbonyl-3-methyl-6,N-bis(trisopropylsilyl)aniline

: 126494-77-7
2,3-dimethyl-N-(phenylsulfonyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / KF; HCl; water / methanol / 2 h / Heating

2: 75 percent / Red-Al / toluene / 3 h / Heating

3: 97 percent / pyridine / CH₂Cl₂

With pyridine; hydrogenchloride; potassium fluoride; water; sodium bis(2-methoxyethoxy)aluminium dihydride; In methanol; dichloromethane; toluene;
DOI:10.1002/1099-0690(200207)2002:13<2094::AID-EJOC2094>3.0.CO;2-E

Reference yield:

: 18595-13-6
2-amino-6-methylbenzoic acid methyl ester

: 126494-77-7
2,3-dimethyl-N-(phenylsulfonyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Red-Al / toluene / 3 h / Heating

2: 97 percent / pyridine / CH₂Cl₂

With pyridine; sodium bis(2-methoxyethoxy)aluminium dihydride; In dichloromethane; toluene;
DOI:10.1002/1099-0690(200207)2002:13<2094::AID-EJOC2094>3.0.CO;2-E