(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

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Chemical Name:(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate
CAS No.:1355150-05-8
Molecular Formula:C₃₂H₃₀BrN₃O₇
Molecular Weight:648.51
Hs Code.:

Synonyms:(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

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Chemical Property of (4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

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Technology Process of (4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

There total 1 articles about (4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 629-03-8
1 ,6-dibromohexane

: 1355150-04-7
C₂₆H₁₉N₃O₇

: 1355150-05-8
(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; at 90 ℃; for 18h;
DOI:10.1002/cbic.201100522

Reference yield:

: 1355150-05-8
(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

: C₄₅H₅₀N₆O₈

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 18 h / Reflux

2: thiophenol / acetonitrile / 2 h / 80 °C

With potassium carbonate; thiophenol; In acetonitrile; 1: Williamson reaction;
DOI:10.1002/cbic.201100522

Reference yield:

: 1355150-05-8
(4-nitrophenyl)methyl 3-{5-[(6-bromohexyl)oxy]-1H-indol-3-yl}-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoate

: 1355150-07-0
3-[5-({6-[(4-{[2-(diethylamino)ethyl]carbamoyl}phenyl)amino]-hexyl}oxy)-1H-indol-3-yl]-2-(1,3-dioxo-2,3-dihydro-1H-isoindol-2-yl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 18 h / Reflux

2: thiophenol / acetonitrile / 2 h / 80 °C

3: water / acetonitrile / 0.5 h / 80 °C

With water; potassium carbonate; thiophenol; In acetonitrile; 1: Williamson reaction;
DOI:10.1002/cbic.201100522