N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

Base Information

Chemical Name:N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride
CAS No.:1374427-45-8
Molecular Formula:C₁₇H₂₆N₂Si*ClH
Molecular Weight:322.953
Hs Code.:

Synonyms:N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

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Chemical Property of N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

Chemical Property:

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Technology Process of N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

There total 4 articles about N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374427-03-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

: 1374427-45-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 25 ℃; for 0.5h;

Reference yield:

: 1374427-95-8
2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)aniline

: 1374427-45-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / 12 h / Reflux

1.2: 12 h / 25 °C

2.1: hydrogenchloride / diethyl ether / 0.5 h / 25 °C

With hydrogenchloride; toluene-4-sulfonic acid; In diethyl ether;

Reference yield:

: 117832-13-0
2,5-dimethyl-4-iodoaniline

: 1374427-45-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 15 h / 50 °C

2.1: toluene-4-sulfonic acid / 12 h / Reflux

2.2: 12 h / 25 °C

3.1: hydrogenchloride / diethyl ether / 0.5 h / 25 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; diethyl ether;