N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

Base Information

Chemical Name:N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine
CAS No.:1374427-03-8
Molecular Formula:C₁₇H₂₆N₂Si
Molecular Weight:286.492
Hs Code.:

Synonyms:N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

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Chemical Property of N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

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Technology Process of N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

There total 3 articles about N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-78-2
N-Ethylmethylamine

: 1374427-95-8
2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)aniline

: 149-73-5
trimethyl orthoformate

: 1374427-03-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

Guidance literature:: 2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)aniline; trimethyl orthoformate; With toluene-4-sulfonic acid; for 12h; Reflux;

N-Ethylmethylamine; In dichloromethane; at 25 ℃; for 12h;

Reference yield:

: 117832-13-0
2,5-dimethyl-4-iodoaniline

: 1374427-03-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 15 h / 50 °C

2.1: toluene-4-sulfonic acid / 12 h / Reflux

2.2: 12 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran;

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 1374427-03-8
N-ethyl-N-methyl-N′-[2,5-dimethyl-4-(2-trimethylsilyl-1-ethynyl)phenyl]formamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 15 h / 50 °C

2.1: toluene-4-sulfonic acid / 12 h / Reflux

2.2: 12 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran;