N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

Base Information

Chemical Name:N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid
CAS No.:77483-52-4
Molecular Formula:C₂₆H₃₃NO₇
Molecular Weight:471.551
Hs Code.:

Synonyms:N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

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Technology Process of N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

There total 2 articles about N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

: 77483-51-3
3-Benzylamino-4-(3,4-dimethoxyphenyl)-buttersaeureethylester

: 36239-09-5
ethyl chlorocarbonylacetate

: 77483-52-4
N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

Guidance literature:: With N,N-dimethyl-aniline; In diethyl ether; for 3h; Heating;
DOI:10.1002/ardp.19813140106

Reference yield:

: 77483-48-8
3-Benzylamino-4-(3,4-dimethoxyphenyl)-isocrotonsaeureethylester

: 77483-52-4
N-Benzyl-N-<3-(3,4-dimethoxyphenyl)-1-ethoxycarbonyl-2-propyl>-malonsaeureethylesteramid

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / H₂ / 10percent Pd/C / ethyl acetate / 72 h / Ambient temperature

2: 74.6 percent / N,N-dimethylaniline / diethyl ether / 3 h / Heating

With hydrogen; N,N-dimethyl-aniline; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1002/ardp.19813140106