C₂₇H₃₀NOP

Base Information

Chemical Name:C₂₇H₃₀NOP
CAS No.:1350923-74-8
Molecular Formula:C₂₇H₃₀NOP
Molecular Weight:415.515
Hs Code.:

Synonyms:C₂₇H₃₀NOP

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₀NOP

Chemical Property:

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Technology Process of C₂₇H₃₀NOP

There total 7 articles about C₂₇H₃₀NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1350923-79-3
(S)-2-(2-bromophenyl)-4-isobutyl-5,5-dimethyl-4,5-dihydrooxazole

: 829-85-6
diphenylphosphane

: 1350923-74-8
C₂₇H₃₀NOP

Guidance literature:: With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In toluene; at 20 - 110 ℃; Inert atmosphere;
DOI:10.1021/jo2019653

Reference yield:

: 1350923-76-0
2-bromo-N-((S)-2-hydroxy-2,5-dimethylhexan-3-yl)benzamide

: 1350923-74-8
C₂₇H₃₀NOP

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid / dichloromethane / 0 - 40 °C / Inert atmosphere

2: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / toluene / 20 - 110 °C / Inert atmosphere

With copper(l) iodide; methanesulfonic acid; caesium carbonate; N,N`-dimethylethylenediamine; In dichloromethane; toluene; 2: Ullmann type reaction;
DOI:10.1021/jo2019653

Reference yield:

: 944141-90-6
C₈H₁₉NO

: 1350923-74-8
C₂₇H₃₀NOP

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / 1,4-dioxane / 2 h / 0 °C / Inert atmosphere

2: methanesulfonic acid / dichloromethane / 0 - 40 °C / Inert atmosphere

3: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / toluene / 20 - 110 °C / Inert atmosphere

With copper(l) iodide; methanesulfonic acid; caesium carbonate; triethylamine; N,N`-dimethylethylenediamine; In 1,4-dioxane; dichloromethane; toluene; 3: Ullmann type reaction;
DOI:10.1021/jo2019653