4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

Base Information

Chemical Name:4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate
CAS No.:1423166-15-7
Molecular Formula:C₂₀H₁₆N₂O₇S₃
Molecular Weight:492.554
Hs Code.:

Synonyms:4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

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Chemical Property of 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

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Technology Process of 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

There total 10 articles about 4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₅H₂₄N₂O₉S₃

: 1423166-15-7
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2016.03.012

Reference yield:

: 1423166-20-4
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-azido-2-((4-(nitrooxy)butanoyl)oxy)benzoate

: 1423166-15-7
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: With methanol; In tetrahydrofuran;

Reference yield:

: 18274-81-2
desmethyl anethole trithione

: 1423166-15-7
4-(3-thioxo-3H-1,2-dithiol-5-yl)phenyl 5-amino-2-((4-(nitrooxy)butanoyl)oxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

3: silver nitrate / acetonitrile / 3 h / 70 °C / Darkness

4: hydrogenchloride / dichloromethane / 1 h / 20 °C

With hydrogenchloride; dmap; silver nitrate; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2016.03.012