Technology Process of C24H34O7
There total 7 articles about C24H34O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 14h;
Inert atmosphere;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere
2: camphor-10-sulfonic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
With
camphor-10-sulfonic acid; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 3 steps
1: magnesium bromide ethyl etherate / toluene / 1.17 h / -78 - 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere
3: camphor-10-sulfonic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
With
camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; magnesium bromide ethyl etherate;
In
tetrahydrofuran; dichloromethane; toluene;
1: Mukaiyama aldol reaction;
DOI:10.1002/anie.201103270