3,4-Dimethylbenzyl bromide

Base Information

Chemical Name:3,4-Dimethylbenzyl bromide
CAS No.:94416-66-7
Molecular Formula:C9H11 Br
Molecular Weight:199.09
Hs Code.:2903999090
European Community (EC) Number:821-918-5
DSSTox Substance ID:DTXSID70526808
Nikkaji Number:J944.174C
Wikidata:Q72469486
Mol file:94416-66-7.mol

Synonyms:3,4-Dimethylbenzyl bromide;94416-66-7;4-(bromomethyl)-1,2-dimethylbenzene;3,4-DIMETHYLBENZYLBROMIDE;MFCD06136695;Benzene, 4-(bromomethyl)-1,2-dimethyl-;BENZENE,4-(BROMOMETHYL)-1,2-DIMETHYL-;SCHEMBL539541;DTXSID70526808;ISFQLPGWXMGYKM-UHFFFAOYSA-N;3 pound not4-Dimethylbenzyl bromide;4-bromomethyl-1,2-dimethyl-benzene;AKOS009941556;AM83115;CS-W021802;AS-18622;SY067380;A21308;EN300-1231948

Suppliers and Price of 3,4-Dimethylbenzyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
3,4-Dimethylbenzyl bromide
5 g
$ 830.00

Biosynth Carbosynth
3,4-Dimethylbenzyl bromide
1 g
$ 295.00

Biosynth Carbosynth
3,4-Dimethylbenzyl bromide
500 mg
$ 200.00

Biosynth Carbosynth
3,4-Dimethylbenzyl bromide
250 mg
$ 125.00

Biosynth Carbosynth
3,4-Dimethylbenzyl bromide
2 g
$ 460.00

Ambeed
3,4-Dimethylbenzylbromide 97%
5g
$ 375.00

Ambeed
3,4-Dimethylbenzylbromide 97%
1g
$ 102.00

Ambeed
3,4-Dimethylbenzylbromide 97%
250mg
$ 42.00

Ambeed
3,4-Dimethylbenzylbromide 97%
10g
$ 593.00

Alichem
3,4-Dimethylbenzylbromide
500mg
$ 806.85

Total 24 raw suppliers

Chemical Property of 3,4-Dimethylbenzyl bromide

Chemical Property:

Boiling Point:237.4±9.0℃ (760 Torr)
Flash Point:103.2±11.8℃
PSA：0.00000
Density:1.314±0.06 g/cm3 (20 ºC 760 Torr)
LogP:3.19830
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:198.00441
Heavy Atom Count:10
Complexity:101

Purity/Quality:

99%, ^*data from raw suppliers

3,4-Dimethylbenzyl bromide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)CBr)C

Technology Process of 3,4-Dimethylbenzyl bromide

There total 5 articles about 3,4-Dimethylbenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 6966-10-5
3,4-dimethylbenzyl alcohol

: 94416-66-7
3,4-dimethylbenzyl bromide

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 ℃;
DOI:10.1039/b306878a

Reference yield: 58.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 95-47-6
o-xylene

: 94416-66-7
3,4-dimethylbenzyl bromide

Guidance literature:: With hydrogen bromide; In acetic acid; at 50 ℃; for 2h;

Reference yield:

: 619-04-5
3,4-dimethylbenzoic acid

: 94416-66-7
3,4-dimethylbenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 0 °C / r.t., overnight

2: PPh₃; CBr₄ / CH₂Cl₂ / 2 h / reflux

With lithium aluminium tetrahydride; carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; dichloromethane; 1: Reduction / 2: Substitution;
DOI:10.1002/1526-4998(200010)56:10<875::AID-PS220>3.0.CO;2-A