cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside

Base Information

• Chemical Name: cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside
• CAS No.: 1611474-43-1
• Molecular Formula: C₃₃H₃₄O₉
• Molecular Weight: 574.628
• Mol file: 1611474-43-1.mol

Synonyms:cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside

Chemical Property of cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside

There total 8 articles about cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C48H44O11 (1611474-42-0) → cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside (1611474-43-1)

Guidance literature:

With triethylamine; In pyridine; at 20 ℃; Inert atmosphere;

DOI:10.3390/molecules19022602

Reference yield: 94.0%

C39H48O9Si → cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside (1611474-43-1)

Guidance literature:

With pyridine hydrogenfluoride; In acetonitrile; at 25 ℃; for 1h; Inert atmosphere;

DOI:10.1002/anie.201914557

Reference yield:

2,3,4-tri-o-benzoyl-6-O-9-fluorenylmethyloxycarboxyl-α-D-glucopyranosyl bromide (1611474-34-0) → cyclohexyl 2,3,4-tri-O-benzoyl-β-D-galactopyranoside (1611474-43-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: mercury(II) cyanide / toluene / 100 °C / Inert atmosphere; Molecular sieve

2.1: tetrabutylammonium perchlorate / 1,2-dichloro-ethane / 40 °C / Inert atmosphere; Molecular sieve; Electrolysis

2.2: Inert atmosphere; Molecular sieve

3.1: triethylamine / pyridine / 20 °C / Inert atmosphere

With tetrabutylammonium perchlorate; mercury(II) cyanide; triethylamine; In pyridine; 1,2-dichloro-ethane; toluene;

DOI:10.3390/molecules19022602

upstream raw materials:

D-Glucose

benzoyl chloride

1,2,3,4-tetra-O-benzoyl-6-O-triphenylmethyl-β-D-glucopyranose

2,3,4-tri-o-benzoyl-6-O-9-fluorenylmethyloxycarboxyl-α-D-glucopyranosyl bromide

Downstream raw materials:

C₇₅H₆₆O₁₉