(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Base Information

Chemical Name:(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide
CAS No.:1068142-14-2
Molecular Formula:C₂₈H₂₇F₁₇N₂O₅S₂
Molecular Weight:858.638
Hs Code.:

Synonyms:(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Suppliers and Price of (S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Useful:

Technology Process of (S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

There total 8 articles about (S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1068142-18-6
(S)-N-{1-azido-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyloxy)phenyl]prop-2-yl} methanesulfonamide

: 98-59-9
p-toluenesulfonyl chloride

: 1068142-14-2
(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Guidance literature:: (S)-N-{1-azido-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyloxy)phenyl]prop-2-yl} methanesulfonamide; With hydrogen; palladium on activated charcoal; In 1,4-dioxane;

p-toluenesulfonyl chloride; With pyridine; at 20 ℃; for 3h; Further stages.;
DOI:10.1016/j.tetlet.2008.07.125

Reference yield:

: C₂₁H₂₁F₁₇N₂O₃S

: 98-59-9
p-toluenesulfonyl chloride

: 1068142-14-2
(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Guidance literature:: With pyridine; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2015.09.024

Reference yield:

: 1068142-18-6
(S)-N-{1-azido-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyloxy)phenyl]prop-2-yl} methanesulfonamide

: 1068142-14-2
(S)-N-{3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl}-4-toluenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / 1,4-dioxane / 17 h / 20 °C

2: pyridine / 3 h / 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In 1,4-dioxane;
DOI:10.1016/j.tet.2015.09.024