(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

Base Information

Chemical Name:(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate
CAS No.:1075706-14-7
Molecular Formula:C₂H₄O₂*C₁₈H₂₁N₃O₄
Molecular Weight:403.435
Hs Code.:

Synonyms:(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

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Chemical Property of (R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

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Technology Process of (R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

There total 1 articles about (R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 635712-55-9
(R)-2-benzyloxycarbonylamino-3-(3,4-dinitro-phenyl)-propionic acid methyl ester

: 64-19-7,77671-22-8
acetic acid

: 1075706-14-7
(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

Guidance literature:: (R)-2-benzyloxycarbonylamino-3-(3,4-dinitro-phenyl)-propionic acid methyl ester; With ammonium formate; zinc; In methanol; at 0 - 20 ℃;

acetic acid; In ethyl acetate; toluene;
DOI:10.1021/jo801577t

Reference yield: 95.0%

: 1075706-14-7
(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

: 64-19-7,77671-22-8
acetic acid

: 635712-58-2
(R)-2-benzyloxycarbonylamino-3-(2-methyl-1H-benzoimidazol-5-yl)-propionic acid methyl ester

Guidance literature:: at 130 ℃; for 4h;
DOI:10.1021/jo801577t

Reference yield: 94.0%

: 1075706-14-7
(R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate

: 635712-70-8
3-(1H-benzotriazol-5-yl)-2-benzyloxycarbonylamino-propionic acid methyl ester

Guidance literature:: (R)-2-benzyloxycarbonylamino-3-(3,4-diamino-phenyl)-propionic acid methyl ester acetate; With acetic acid; sodium nitrite; In water; at 20 ℃; for 0.333333h;

With ammonium hydroxide; In water; pH=11; optical yield given as %ee;
DOI:10.1021/jo801577t