(S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

Base Information

Chemical Name:(S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride
CAS No.:182305-29-9
Molecular Formula:C₂₀H₃₃GeNO*ClH
Molecular Weight:412.539
Hs Code.:

Synonyms:(S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

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Chemical Property of (S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

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Technology Process of (S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

There total 1 articles about (S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: 180613-39-2
rac-cyclohexyl(hydroxymethyl)phenyl(2-piperidinoethyl)germane

: 182305-29-9
(S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

Guidance literature:: With (S,S)-O,O'-di-p-toluyltartaric acid; NaOH; In acetone; N2-atmosphere; mixing germane with tartaric acid derivative in boiling acetone, crystn. (room temp., 60 h), multistep fractional crystn. (Me2CO), treatment with 2 M NaOH in water/Et2O, sepn. of org. layer, evapn., stirring with HCl in ether; evapn. (reduced pressure), drying (vac.), recrystn. (Et2O diffusion intoMe2CO soln.); elem. anal.;
DOI:10.1016/0022-328X(96)06300-0

Reference yield: 93.0%

: 182305-29-9
(S)-1-(2-[cyclohexyl(hydroxymethyl)phenylgermyl]ethyl)piperidinium chloride

: 165657-85-2
(S)-cyclohexyl(hydroxymethyl)phenyl(2-piperidinoethyl)germane

Guidance literature:: With NaOH; In diethyl ether; water; N2-atmosphere; addn. of aq. NaOH to hydrochloride (in water/Et2O), stirring for 5 min; extn. of aq. layer (Et2O), drying combined org. layers (Na2SO4), solventremoval (reduced pressure), drying (vac.); elem. anal.;
DOI:10.1016/0022-328X(96)06300-0