C₂₆H₄₈O₅Si₂

Base Information

Chemical Name:C₂₆H₄₈O₅Si₂
CAS No.:1422462-85-8
Molecular Formula:C₂₆H₄₈O₅Si₂
Molecular Weight:496.835
Hs Code.:

C<sub>26</sub>H<sub>48</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₂₆H₄₈O₅Si₂

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Chemical Property of C₂₆H₄₈O₅Si₂

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Technology Process of C₂₆H₄₈O₅Si₂

There total 6 articles about C₂₆H₄₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1422463-16-8
C₂₃H₄₀O₅Si

: 1422462-85-8
C₂₆H₄₈O₅Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/jo3026077

Reference yield:

: 866148-48-3
(2R,3S,4R,6R)-2-(4-Methoxy-benzyloxy)-4-methyl-3,6-bis-triethylsilanyloxy-heptanethioic acid S-ethyl ester

: 1422462-85-8
C₂₆H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide / diethyl ether / 0.25 h / 0 °C / Inert atmosphere

1.2: 2 h / -50 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 2.17 h / 0 - 5 °C

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2.17 h / 0 - 20 °C

4.1: methanol; barium hydroxide octahydrate / 1 h

5.1: 2,6-dimethylpyridine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; methanol; copper(l) iodide; barium hydroxide octahydrate; water; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; 3.1: |Mitsunobu Displacement;
DOI:10.1021/jo3026077

Reference yield:

: C₃₈H₆₁NO₇Si₂

: 1422462-85-8
C₂₆H₄₈O₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 °C / Inert atmosphere

1.2: 0.33 h / 0 °C / Inert atmosphere

2.1: copper(l) iodide / diethyl ether / 0.25 h / 0 °C / Inert atmosphere

2.2: 2 h / -50 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 2.17 h / 0 - 5 °C

4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2.17 h / 0 - 20 °C

5.1: methanol; barium hydroxide octahydrate / 1 h

6.1: 2,6-dimethylpyridine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

With 2,6-dimethylpyridine; methanol; copper(l) iodide; n-butyllithium; barium hydroxide octahydrate; water; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; 4.1: |Mitsunobu Displacement;
DOI:10.1021/jo3026077