Technology Process of C18H19BrO
There total 4 articles about C18H19BrO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Oxone; Shi's ketone; Na2B4O7*10H2O; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate;
In
acetonitrile;
at 0 ℃;
for 3h;
enantioselective reaction;
DOI:10.1055/s-0033-1340825
- Guidance literature:
-
Multi-step reaction with 3 steps
1: magnesium; iodine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: hydrogenchloride / ethanol / Reflux
3: Shi's ketone; Na2B4O7*10H2O; potassium carbonate; Oxone; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 3 h / 0 °C
With
hydrogenchloride; Oxone; Shi's ketone; Na2B4O7*10H2O; iodine; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; magnesium;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1055/s-0033-1340825
- Guidance literature:
-
Multi-step reaction with 3 steps
1: magnesium; iodine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: hydrogenchloride / ethanol / Reflux
3: Shi's ketone; Na2B4O7*10H2O; potassium carbonate; Oxone; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 3 h / 0 °C
With
hydrogenchloride; Oxone; Shi's ketone; Na2B4O7*10H2O; iodine; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; magnesium;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1055/s-0033-1340825