2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

Base Information

Chemical Name:2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde
CAS No.:1307812-92-5
Molecular Formula:C₂₆H₂₄FNO₂
Molecular Weight:401.48
Hs Code.:

Synonyms:2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

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Chemical Property of 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

Chemical Property:

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Technology Process of 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

There total 12 articles about 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1307812-91-4
1-(2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazol-7-yl)ethane-1,2-diol

: 1307812-92-5
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

Guidance literature:: With sodium periodate; In methanol; water; at 0 ℃; for 0.5h;

Reference yield:

: 3470-50-6
6-Hydroxy-1-tetralone

: 1307812-92-5
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 4 h / 0 - 20 °C

2: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

3: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

4: dmap / 1,2-dichloro-benzene / 0.17 h / 180 °C / Microwave irradiation

5: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tetrahydrofuran / 18 h / 20 °C

6: sodium periodate / water; methanol / 0.5 h / 0 °C

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; hydroxylamine hydrochloride; sodium acetate; 4-methylmorpholine N-oxide; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; water; 1,2-dichloro-benzene;

Reference yield:

: 144464-64-2
5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl trifluoromethanesulfonate

: 1307812-92-5
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)naphtho[1,2-d]oxazole-7-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

3: dmap / 1,2-dichloro-benzene / 0.17 h / 180 °C / Microwave irradiation

4: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tetrahydrofuran / 18 h / 20 °C

5: sodium periodate / water; methanol / 0.5 h / 0 °C

With dmap; sodium periodate; osmium(VIII) oxide; hydroxylamine hydrochloride; sodium acetate; 4-methylmorpholine N-oxide; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; methanol; water; 1,2-dichloro-benzene;