5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride

Base Information

• Chemical Name: 5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride
• CAS No.: 1395885-06-9
• Molecular Formula: C₂₀H₁₉N₅O₄*ClH
• Molecular Weight: 429.863

Synonyms:5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride

Chemical Property of 5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride

Chemical Property:

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Technology Process of 5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride

There total 1 articles about 5-amino-N⁴-(2-carboxyphenyl)-N²-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

N4-(2-carboxyphenyl)-2-chloropyrimidine-4,5-diamine hydrochloride (1395886-60-8) + p-aminoethylbenzoate (94-09-7) → 5-amino-N4-(2-carboxyphenyl)-N2-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride (1395885-06-9)

Guidance literature:

In 1,4-dioxane; iso-butanol; at 120 ℃; for 24h; Sealed tube;

DOI:10.1021/jm300334d

Reference yield: 65.0%

5-amino-N4-(2-carboxyphenyl)-N2-(4-ethoxycarbonylphenyl)pyrimidine-2,4-diamine hydrochloride (1395885-06-9) → 5-amino-N4-(2'-carboxyphenyl)-N2-(4'-carboxyphenyl)pyrimidine-2,4-diamine (1395885-15-0)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 100 ℃; for 0.5h; Sealed tube;

DOI:10.1021/jm300334d

upstream raw materials:

N⁴-(2-carboxyphenyl)-2-chloropyrimidine-4,5-diamine hydrochloride

p-aminoethylbenzoate

Downstream raw materials:

5-amino-N₄-(2'-carboxyphenyl)-N₂-(4'-carboxyphenyl)pyrimidine-2,4-diamine

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