1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

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Chemical Name:1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose
CAS No.:291776-21-1
Molecular Formula:C₃₄H₃₁NO₆
Molecular Weight:549.623
Hs Code.:

Synonyms:1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

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Chemical Property of 1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

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Technology Process of 1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

There total 5 articles about 1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98-88-4
benzoyl chloride

: 84034-62-8
N-((1R,2S,3R,4R,5R)-3-hydroxy-2-(trityloxy)-6,8-dioxabicyclo[3.2.1]octan-4-yl)acetamide

: 291776-21-1
1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1007/BF02758670

Reference yield:

: 37042-52-7
N-((1R,2S,3R,4R,5R)-2,3-dihydroxy-6,8-dioxabicyclo[3.2.1]octan-4-yl)acetamide

: 291776-21-1
1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 2,4,6-collidine / CH₂Cl₂ / 2 h / 20 °C

2: 89 percent / pyridine / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; In dichloromethane; 1: tritylation / 2: Acylation;
DOI:10.1007/BF02758670

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 291776-21-1
1,6-anhydro-2-acetamido-3-O-benzoyl-2-deoxy-4-O-trityl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂

2: 2,4,6-collidine / CH₂Cl₂ / 2 h / 20 °C

3: 89 percent / pyridine / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; In dichloromethane; 1: Esterification / 2: tritylation / 3: Acylation;
DOI:10.1007/BF02758670