trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

Base Information

Chemical Name:trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene
CAS No.:133970-15-7
Molecular Formula:C₂₆H₂₆Cl₂N₂O
Molecular Weight:453.411
Hs Code.:

Synonyms:trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

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Chemical Property of trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

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Technology Process of trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

There total 4 articles about trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 133970-13-5
trans-2-pyrrolidinyl-3-(methylamino)-1,2,3,4-tetrahydroanthracene

: 3024-72-4
3,4-dichlorobenzoyl chloride

: 133970-15-7
trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

Guidance literature:: With triethylamine; In diethyl ether; for 18h; Ambient temperature;
DOI:10.1021/jm00110a021

Reference yield:

: 5910-32-7
1,4-dihydroanthracene

: 133970-15-7
trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

Guidance literature:: Multi-step reaction with 4 steps

1: 3-chloroperoxybenzoic acid / CHCl₃ / 0.58 h / Ambient temperature

2: 16 h / 95 °C

3: 1.) triethylamine, methanesulfonyl chloride / 1.) CH₂Cl₂, 0 deg C, 1.5 h, 2.) 70 deg C, 18 h

4: 75 percent / triethylamine / diethyl ether / 18 h / Ambient temperature

With methanesulfonyl chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; chloroform;
DOI:10.1021/jm00110a021

Reference yield:

: 176236-88-7
2,3-epoxy-1,2,3,4-tetrahydroanthracene

: 133970-15-7
trans-2-pyrrolidinyl-3-(N-methyl-3',4'-dichlorobenzamido)-1,2,3,4-tetrahydroanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 16 h / 95 °C

2: 1.) triethylamine, methanesulfonyl chloride / 1.) CH₂Cl₂, 0 deg C, 1.5 h, 2.) 70 deg C, 18 h

3: 75 percent / triethylamine / diethyl ether / 18 h / Ambient temperature

With methanesulfonyl chloride; triethylamine; In diethyl ether;
DOI:10.1021/jm00110a021