3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

Base Information

Chemical Name:3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid
CAS No.:1289220-86-5
Molecular Formula:C₁₁H₁₃FN₃O₄P
Molecular Weight:301.214
Hs Code.:

Synonyms:3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

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Technology Process of 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

There total 2 articles about 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1289220-64-9
diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

: 1289220-86-5
3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 24h; Darkness; Inert atmosphere;
DOI:10.1080/10426507.2010.494646

Reference yield:

: 2561-17-3
1-ethynyl-3-fluoro-benzene

: 1289220-86-5
3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

2: trimethylsilyl bromide / dichloromethane / 24 h / 20 °C / Darkness; Inert atmosphere

With copper(ll) sulfate pentahydrate; trimethylsilyl bromide; sodium L-ascorbate; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1080/10426507.2010.494646