diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

Base Information

Chemical Name:diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate
CAS No.:1289220-64-9
Molecular Formula:C₁₅H₂₁FN₃O₄P
Molecular Weight:357.322
Hs Code.:

Synonyms:diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

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Technology Process of diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

There total 2 articles about diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2561-17-3
1-ethynyl-3-fluoro-benzene

: 640280-99-5
diethyl (3-azido-2-hydroxypropyl)phosphonate

: 1289220-64-9
diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1080/10426507.2010.494646

Reference yield:

: 7316-37-2
diethyl (oxiran-2-ylmethyl)phosphonate

: 1289220-64-9
diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium sulfate; sodium azide / methanol / 4 h / 65 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C

With ammonium sulfate; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; water; tert-butyl alcohol;
DOI:10.1080/10426507.2010.494646

Reference yield: 83.0%

: 1289220-64-9
diethyl 3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonate

: 1289220-86-5
3-[4-(3-fluorophenyl)-1,2,3-triazol-1-yl]-2-hydroxypropylphosphonic acid

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 24h; Darkness; Inert atmosphere;
DOI:10.1080/10426507.2010.494646