tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

Base Information

Chemical Name:tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate
CAS No.:1268616-40-5
Molecular Formula:C₃₉H₅₁ClO₅S
Molecular Weight:667.35
Hs Code.:

Synonyms:tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

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Chemical Property of tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

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Technology Process of tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

There total 1 articles about tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 20487-40-5
tert-butyl propionate

: 1268616-36-9
3,3-bis(3-phenylpropoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane

: 1268616-40-5
tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

Guidance literature:: tert-butyl propionate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h; Inert atmosphere;

3,3-bis(3-phenylpropoxymethyl)-1-[chloro(p-tolylsulfinyl)methylidene]cyclobutane; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2010.12.023

Reference yield: 84.0%

: 1268616-40-5
tert-butyl 2-(1-[chloro(p-tolylsulfinyl)methyl]-3,3-bis(3-phenylpropoxymethyl)cyclobutyl)propionate

: 1268616-46-1
tert-butyl 2-[4,4-bis(3-phenylpropoxymethyl)cyclopent-1-enyl]propionate

Guidance literature:: With isopropylmagnesium chloride; In diethyl ether; toluene; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.12.023