C₈₃H₁₁₈I₂O₁₀

Base Information

Chemical Name:C₈₃H₁₁₈I₂O₁₀
CAS No.:1618096-64-2
Molecular Formula:C₈₃H₁₁₈I₂O₁₀
Molecular Weight:1529.65
Hs Code.:

C<sub>83</sub>H<sub>118</sub>I<sub>2</sub>O<sub>10</sub>

Synonyms:C₈₃H₁₁₈I₂O₁₀

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Chemical Property of C₈₃H₁₁₈I₂O₁₀

Chemical Property:

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Technology Process of C₈₃H₁₁₈I₂O₁₀

There total 29 articles about C₈₃H₁₁₈I₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.9%

: 1618093-05-2
diethyl 5-((2-ethylhexyl)oxy)-4-iodo-2-methoxybenzylphosphonate

: 1618096-68-6
C₆₇H₉₅IO₉

: 1618096-64-2
C₈₃H₁₁₈I₂O₁₀

Guidance literature:: diethyl 5-((2-ethylhexyl)oxy)-4-iodo-2-methoxybenzylphosphonate; C₆₇H₉₅IO₉; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With iodine; In toluene; Inert atmosphere; Reflux;
DOI:10.1021/jo501266g

Reference yield:

: 63272-66-2
4-bromo-2-hydroxy-5-methoxybenzaldehyde

: 1618096-64-2
C₈₃H₁₁₈I₂O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene-4-sulfonic acid / toluene / Inert atmosphere; Dean-Stark; Reflux

2.1: potassium hydroxide / dimethyl sulfoxide / 50 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / tetrahydrofuran / 0 °C / Inert atmosphere

5.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

6.1: 2 h / 140 °C / Inert atmosphere

7.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

8.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

8.2: Inert atmosphere; Reflux

9.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

10.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

10.2: Inert atmosphere; Reflux

11.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

11.2: Inert atmosphere; Reflux

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; potassium tert-butylate; water; toluene-4-sulfonic acid; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; hexane; dimethyl sulfoxide; toluene; 2.1: |Williamson Ether Synthesis / 7.1: |Horner-Wadsworth-Emmons Olefination / 9.1: |Horner-Wadsworth-Emmons Olefination / 11.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g

Reference yield:

: 1618092-84-4
5-bromo-2-(5,5-dimethyl-1,3-dioxan-2-yl)-4-methoxyphenol

: 1618096-64-2
C₈₃H₁₁₈I₂O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 50 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Glovebox; Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran / 0 °C / Inert atmosphere

4.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

5.1: 2 h / 140 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

7.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

7.2: Inert atmosphere; Reflux

8.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

9.1: water; hydrogenchloride / tetrahydrofuran / 50 °C / Inert atmosphere

9.2: Inert atmosphere; Reflux

10.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

10.2: Inert atmosphere; Reflux

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; carbon tetrabromide; potassium tert-butylate; water; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; hexane; dimethyl sulfoxide; 1.1: |Williamson Ether Synthesis / 6.1: |Horner-Wadsworth-Emmons Olefination / 8.1: |Horner-Wadsworth-Emmons Olefination / 10.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501266g