Boc-Ala-Lys2(Cl)>-Pro

Base Information

Chemical Name:Boc-Ala-Lys2(Cl)>-Pro
CAS No.:111104-01-9
Molecular Formula:C₂₇H₃₉ClN₄O₈
Molecular Weight:583.082
Hs Code.:

Synonyms:Boc-Ala-Lys2(Cl)>-Pro

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Chemical Property of Boc-Ala-Lys2(Cl)>-Pro

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Technology Process of Boc-Ala-Lys2(Cl)>-Pro

There total 6 articles about Boc-Ala-Lys2(Cl)>-Pro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 111104-00-8
Boc-Ala-Lys2(Cl)>-Pro ethyl ester

: 111104-01-9
Boc-Ala-Lys2(Cl)>-Pro

Guidance literature:: With sodium hydroxide; In ethanol; for 4h; Ambient temperature;

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 111104-01-9
Boc-Ala-Lys2(Cl)>-Pro

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine; 2.) DCCI / 2.) 0 deg C, 20 min, chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

2: 93 percent / 1 M NaOH / ethanol / 4 h / Ambient temperature

With 4-methyl-morpholine; sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol;

Reference yield:

: 33305-75-8,131477-20-8
L-proline ethyl ester monohydrochloride

: 111104-01-9
Boc-Ala-Lys2(Cl)>-Pro

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) diluted sulphuric acid, N-methylmorpholine; 2.) DCCI / 1.) H₂O; 2.) 0 deg C, 20 min, chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

2: 1.) 6 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

3: 1.) N-methylmorpholine; 2.) DCCI / 2.) 0 deg C, 20 min, chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

4: 93 percent / 1 M NaOH / ethanol / 4 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; sulfuric acid; dicyclohexyl-carbodiimide; In ethanol;