2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

Base Information

Chemical Name:2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride
CAS No.:1269124-00-6
Molecular Formula:C₁₃H₃Cl₃F₁₀O₄
Molecular Weight:519.507
Hs Code.:

Synonyms:2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

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Chemical Property of 2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

Chemical Property:

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Technology Process of 2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

There total 3 articles about 2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 1269266-95-6
2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthalic acid

: 1269124-00-6
2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

Guidance literature:: With thionyl chloride; Inert atmosphere; Reflux;

Reference yield:

: 1623-05-8
perfluoro(propyl vinyl ether)

: 1269124-00-6
2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate; tetrachloromethane / N,N-dimethyl-formamide / 24 h / 25 °C

2.1: potassium hydroxide; water / Reflux

2.2: 25 °C / pH ~ 1

3.1: thionyl chloride / Inert atmosphere; Reflux

With tetrachloromethane; thionyl chloride; potassium tert-butylate; water; potassium hydroxide; In N,N-dimethyl-formamide;

Reference yield:

: 6342-72-9
dimethyl hydroxyterephthalate

: 1269124-00-6
2-(2-chloro-1,1,2-trifluoro-2-(perfluoropropoxy)ethoxy)terephthaloyl dichloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate; tetrachloromethane / N,N-dimethyl-formamide / 24 h / 25 °C

2.1: potassium hydroxide; water / Reflux

2.2: 25 °C / pH ~ 1

3.1: thionyl chloride / Inert atmosphere; Reflux

With tetrachloromethane; thionyl chloride; potassium tert-butylate; water; potassium hydroxide; In N,N-dimethyl-formamide;