5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

Base Information

Chemical Name:5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide
CAS No.:1026529-66-7
Molecular Formula:C₂₈H₃₄N₂O₂
Molecular Weight:430.59
Hs Code.:

Synonyms:5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

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Chemical Property of 5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

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Technology Process of 5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

There total 8 articles about 5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117-34-0
2,2-diphenylacetic acid

: 1026529-66-7
5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Et₃N, ethyl chloroformate / 1) THF, 0 deg C, 30 min, 2) THF, 0 deg C to r.t.

2: 1) POCl₃, 2) NaBH₄ / 1) r.t., 5 h, 2) glyme, r.t., 12 h

3: Et₃N / tetrahydrofuran

4: 1) N₂H₄*H₂O, 2) 10percent HCl / 1) MeOH, reflux, 1 h, 2) MeOH, reflux, 30 min

With hydrogenchloride; sodium tetrahydroborate; chloroformic acid ethyl ester; hydrazine hydrate; triethylamine; trichlorophosphate; In tetrahydrofuran;
DOI:10.1002/ardp.19973301104

Reference yield:

: 31968-58-8
5-(1,3-Dioxoisoindolin-2-yl)valeryl Chloride

: 1026529-66-7
5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran

2: 1) N₂H₄*H₂O, 2) 10percent HCl / 1) MeOH, reflux, 1 h, 2) MeOH, reflux, 30 min

With hydrogenchloride; hydrazine hydrate; triethylamine; In tetrahydrofuran;
DOI:10.1002/ardp.19973301104

Reference yield:

: 1147-76-8
5-(N-phthalimido)pentanoic acid

: 1026529-66-7
5-Amino-pentanoic acid (2,2-diphenyl-ethyl)-[2-(4-methoxy-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2 / CH₂Cl₂ / 2 h / Ambient temperature

2: Et₃N / tetrahydrofuran

3: 1) N₂H₄*H₂O, 2) 10percent HCl / 1) MeOH, reflux, 1 h, 2) MeOH, reflux, 30 min

With hydrogenchloride; oxalyl dichloride; hydrazine hydrate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.19973301104