2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

Base Information

Chemical Name:2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether
CAS No.:77798-74-4
Molecular Formula:C₃₂H₅₆N₂O₈
Molecular Weight:596.805
Hs Code.:

Synonyms:2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

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Chemical Property of 2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

Chemical Property:

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Technology Process of 2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

There total 9 articles about 2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 77798-73-3
2,5-Bis<11-(methoxycarbonyl)undecyl>-3,6-dinitrohydrochinon-dimethylether

: 77798-74-4
2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

Guidance literature:: With sodium tetrahydroborate; calcium chloride; In tetrahydrofuran; for 48h; Ambient temperature;

Reference yield:

: 1108-58-3
<10-(Methoxycarbonyl)decyl>triphenylphosphoniumiodid

: 77798-74-4
2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

Guidance literature:: Multi-step reaction with 9 steps

1: NaOMe / dimethylformamide / 1) 0 deg C, 10 min, 2) r.t., 1.5 h

2: 70 percent / dimethylformamide / 3 h / Ambient temperature

3: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

4: 48percent HBr / acetic acid / 14 h / 110 °C

5: pyridine / 14 h / Ambient temperature

6: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

7: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

8: 58 percent / K₂CO₃ / acetone / 4 h / Heating

9: 84 percent / CaCl₂, NaBH₄ / tetrahydrofuran / 48 h / Ambient temperature

With sodium tetrahydroborate; sulfur dioxide; hydrogen bromide; hydrogen; nitric acid; sodium methylate; sulphurous acid; potassium carbonate; calcium chloride; nickel; In tetrahydrofuran; pyridine; methanol; acetic acid; propionic acid; N,N-dimethyl-formamide; acetone;

Reference yield:

: 77798-57-3
2,5-Bis(11-methoxycarbonyl-1-undecenyl)hydrochinon-dimethylether

: 77798-74-4
2,5-Bis(12-hydroxydodecyl)-3,6-dinitrohydrochinon-dimethylether

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

2: 48percent HBr / acetic acid / 14 h / 110 °C

3: pyridine / 14 h / Ambient temperature

4: 69 percent / conc. HNO₃ / propionic acid / 240 h / Ambient temperature

5: 8.2 g / H₂SO₃, SO₂ / acetic acid / 5 h / 80 °C

6: 58 percent / K₂CO₃ / acetone / 4 h / Heating

7: 84 percent / CaCl₂, NaBH₄ / tetrahydrofuran / 48 h / Ambient temperature

With sodium tetrahydroborate; sulfur dioxide; hydrogen bromide; hydrogen; nitric acid; sulphurous acid; potassium carbonate; calcium chloride; nickel; In tetrahydrofuran; pyridine; methanol; acetic acid; propionic acid; acetone;