(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

Base Information

Chemical Name:(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]
CAS No.:1005142-91-5
Molecular Formula:C₄₃H₄₃ClO₆
Molecular Weight:691.264
Hs Code.:

Synonyms:(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

Suppliers and Price of (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

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Chemical Property of (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

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Technology Process of (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

There total 1 articles about (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.4%

: C₄₃H₄₄O₇

: 1005142-91-5
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

Guidance literature:: With thionyl chloride; In dichloromethane; at 0 ℃; for 1h;

Reference yield: 47.6%

: 1005142-91-5
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

: 16152-51-5
(4-isopropylphenyl)boronic acid

: 1005142-95-9
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-(benzyloxymethyl)-3',4',5',6'-tetrahydro-6-[(4-isopropylphenyl)methyl]-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; In water; N,N-dimethyl-formamide; at 85 ℃; for 15h;

Reference yield: 41.0%

: 1005142-91-5
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-benzyloxymethyl-6-(chloromethyl)-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

: 87199-17-5
4-formylphenylboronic acid,

: 1005143-07-6
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris(benzyloxy)-6'-(benzyloxymethyl)-6-[(4-formylphenyl)methyl]-3',4',5',6'-tetrahydro-5-methyl-spiro[isobenzofuran-1(3H),2'-[2H]pyran]

Guidance literature:: With tetrabutylammomium bromide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 150 ℃; for 0.333333h; Microwave irradiation;