7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

Base Information

Chemical Name:7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde
CAS No.:1266118-73-3
Molecular Formula:C₂₀H₂₅NO₂
Molecular Weight:311.424
Hs Code.:

Synonyms:7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

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Chemical Property of 7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

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Technology Process of 7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

There total 6 articles about 7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5071-96-5
3-METHOXYBENZYLAMINE

: 1266118-73-3
7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium sulfate; acetic acid / 1.5 h / 20 °C

1.2: 2.67 h

1.3: pH 7

2.1: trifluoroacetic acid / 55 °C / Inert atmosphere

3.1: air / copper(l) iodide / isopropyl alcohol / 54 h / 20 - 55 °C

4.1: boron tribromide / dichloromethane / 2.5 h / 20 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 °C

6.1: selenium(IV) oxide / diphenylether / 4 h / 200 °C / Sealed tube

With selenium(IV) oxide; di-isopropyl azodicarboxylate; boron tribromide; acetic acid; sodium sulfate; triphenylphosphine; trifluoroacetic acid; copper(l) iodide; In diphenylether; dichloromethane; isopropyl alcohol; toluene;

Reference yield:

: 83903-87-1
1,1-dimethoxy-N-(3-methoxybenzyl)propan-2-amine

: 1266118-73-3
7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / 55 °C / Inert atmosphere

2: air / copper(l) iodide / isopropyl alcohol / 54 h / 20 - 55 °C

3: boron tribromide / dichloromethane / 2.5 h / 20 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 °C

5: selenium(IV) oxide / diphenylether / 4 h / 200 °C / Sealed tube

With selenium(IV) oxide; di-isopropyl azodicarboxylate; boron tribromide; triphenylphosphine; trifluoroacetic acid; copper(l) iodide; In diphenylether; dichloromethane; isopropyl alcohol; toluene;

Reference yield:

: 1393451-05-2
C₁₁H₁₃NO

: 1266118-73-3
7-(trans-4-tert-butylcyclohexyloxy)isoquinoline-3-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: air / copper(l) iodide / isopropyl alcohol / 54 h / 20 - 55 °C

2: boron tribromide / dichloromethane / 2.5 h / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 20 °C

4: selenium(IV) oxide / diphenylether / 4 h / 200 °C / Sealed tube

With selenium(IV) oxide; di-isopropyl azodicarboxylate; boron tribromide; triphenylphosphine; copper(l) iodide; In diphenylether; dichloromethane; isopropyl alcohol; toluene;