N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

Base Information

Chemical Name:N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide
CAS No.:107413-68-3
Molecular Formula:C₁₇H₁₃N₃O₅S
Molecular Weight:371.373
Hs Code.:

Synonyms:N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

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Technology Process of N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

There total 5 articles about N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2937-05-5
4-nitrobenzenesulfonohydrazide

: 708-06-5
2-hydroxynaphthalene-1-carbaldehyde

: 107413-68-3
N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: With acetic acid; In methanol; Reflux;
DOI:10.1021/acs.jmedchem.7b00530

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 107413-68-3
N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / CH₂Cl₂ / 0.25 h

2: ethanol / Heating

With hydrazine; In ethanol; dichloromethane;
DOI:10.1128/AAC.46.8.2450-2457.2002

Reference yield:

: 5386-25-4
1-hydroxymethyl-2-naphthol

: 107413-68-3
N'-((2-hydroxynaphthalen-1-yl)methylene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 12 h / 20 °C / Inert atmosphere

2: acetic acid / methanol / Reflux

With acetic acid; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1021/acs.jmedchem.7b00530