C₄₁H₅₄O₈

Base Information

Chemical Name:C₄₁H₅₄O₈
CAS No.:104307-09-7
Molecular Formula:C₄₁H₅₄O₈
Molecular Weight:674.875
Hs Code.:

C<sub>41</sub>H<sub>54</sub>O<sub>8</sub>

Synonyms:C₄₁H₅₄O₈

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Chemical Property of C₄₁H₅₄O₈

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Technology Process of C₄₁H₅₄O₈

There total 20 articles about C₄₁H₅₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 104307-08-6
C₄₁H₅₆O₈

: 104307-09-7
C₄₁H₅₄O₈

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)84149-0

Reference yield:

: 104307-04-2
C₅₁H₇₀O₁₀Si

: 104307-09-7
C₄₁H₅₄O₈

Guidance literature:: Multi-step reaction with 9 steps

1: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

2: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

3: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

4: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

5: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

6: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

7: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

8: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

9: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

With sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0

Reference yield:

: 104307-01-9
C₃₈H₄₈O₈Si

: 104307-09-7
C₄₁H₅₄O₈

Guidance literature:: Multi-step reaction with 12 steps

1: 1) butyllithium / 1) ether, hexane, -42 to 0 deg C, 2) ether, hexane, -42 deg C, 10 min.

2: CrO₃*2pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: aluminum amalgam / tetrahydrofuran / Ambient temperature

4: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

5: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

6: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

7: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

8: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

9: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

10: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

11: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

12: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

With sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; aluminium amalgam; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; dipyridine chromium trioxide; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0