2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

Base Information

Chemical Name:2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one
CAS No.:145694-01-5
Molecular Formula:C₂₀H₁₈N₂O₃S
Molecular Weight:366.441
Hs Code.:

Synonyms:2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

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Chemical Property of 2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

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Technology Process of 2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

There total 5 articles about 2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 105-39-5
chloroacetic acid ethyl ester

: 155496-29-0
2-thioxo-3-phenyl-5-phenylmethylene-4-imidazolidinone

: 145694-01-5
2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

Guidance literature:: With potassium carbonate; In acetonitrile; at 50 ℃; for 2h;
DOI:10.1080/713744555

Reference yield:

: 103-71-9
phenyl isocyanate

: 145694-01-5
2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 20 °C

2: Na₂S*9H₂O; HOAc / acetonitrile / 20 °C

3: 83 percent / potassium carbonate / acetonitrile / 2 h / 50 °C

With sodium sulfide; potassium carbonate; acetic acid; In dichloromethane; acetonitrile; 1: aza-Wittig reaction;
DOI:10.1081/SCC-120018686

Reference yield:

: (Z)-3-Phenyl-2-phenyliminomethyleneamino-acrylic acid ethyl ester

: 145694-01-5
2-ethoxycarbonylmethylthio-3-phenyl-5-phenylmethylene-4H-imidazol-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂S*9H₂O; HOAc / acetonitrile / 20 °C

2: 83 percent / potassium carbonate / acetonitrile / 2 h / 50 °C

With sodium sulfide; potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1081/SCC-120018686