2-azido-5-chlorophenylboronic acid pinacolate ester

Base Information

Chemical Name:2-azido-5-chlorophenylboronic acid pinacolate ester
CAS No.:1611447-03-0
Molecular Formula:C₁₂H₁₅BClN₃O₂
Molecular Weight:279.534
Hs Code.:

Synonyms:2-azido-5-chlorophenylboronic acid pinacolate ester

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Chemical Property of 2-azido-5-chlorophenylboronic acid pinacolate ester

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Technology Process of 2-azido-5-chlorophenylboronic acid pinacolate ester

There total 4 articles about 2-azido-5-chlorophenylboronic acid pinacolate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1073371-77-3
4-chloro-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

: 1611447-03-0
2-azido-5-chlorophenylboronic acid pinacolate ester

Guidance literature:: With 2-Methyl-2-nitropropane; trimethylsilylazide; In acetonitrile; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol5010615

Reference yield:

: 873-38-1
4-chloro-2-bromoaniline

: 1611447-03-0
2-azido-5-chlorophenylboronic acid pinacolate ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 12 h / 120 °C / Inert atmosphere

2: trimethylsilylazide; 2-Methyl-2-nitropropane / acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 2-Methyl-2-nitropropane; trimethylsilylazide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/ol5010615

Reference yield:

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1611447-03-0
2-azido-5-chlorophenylboronic acid pinacolate ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 12 h / 120 °C / Inert atmosphere

2: trimethylsilylazide; 2-Methyl-2-nitropropane / acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 2-Methyl-2-nitropropane; trimethylsilylazide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/ol5010615