3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Base Information

Chemical Name:3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate
CAS No.:1119204-87-3
Molecular Formula:C₂₁H₁₈ClF₂N₃O₃
Molecular Weight:433.842
Hs Code.:

Synonyms:3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

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Chemical Property of 3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

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Technology Process of 3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

There total 6 articles about 3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007098-98-7
2-(3-aminobenzyl)-6-(3,5-difluorophenyl)-2H-pyridazin-3-one

: 628-11-5
3-chloropropyl chloroformate

: 1119204-87-3
3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Guidance literature:: With sodium carbonate; In water; acetone; at 64 ℃;

Reference yield:

: 156545-07-2
3,5-difluorophenylboronic acid

: 1119204-87-3
3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water / 5 h / 100 °C

2: water; formic acid / 18 h / Heating

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 40 - 70 °C

4: hydrogen / palladium on carbon / tetrahydrofuran / 20 °C / 760.05 Torr

5: sodium carbonate / water; acetone / 64 °C

With formic acid; water; hydrogen; sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on carbon; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol; water; acetone;

Reference yield:

: 1007098-93-2
6-(3,5-difluorophenyl)pyridazine-3(2H)-one

: 1119204-87-3
3-chloropropyl {3-[3-(3,5-difluorophenyl)-6-oxo-6H-pyridazin-1-ylmethyl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 6 h / 40 - 70 °C

2: hydrogen / palladium on carbon / tetrahydrofuran / 20 °C / 760.05 Torr

3: sodium carbonate / water; acetone / 64 °C

With hydrogen; sodium carbonate; potassium carbonate; palladium on carbon; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water; acetone;