C₃₀H₃₆O₇

Base Information

Chemical Name:C₃₀H₃₆O₇
CAS No.:942068-64-6
Molecular Formula:C₃₀H₃₆O₇
Molecular Weight:508.612
Hs Code.:

C<sub>30</sub>H<sub>36</sub>O<sub>7</sub>

Synonyms:C₃₀H₃₆O₇

Suppliers and Price of C₃₀H₃₆O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₀H₃₆O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₀H₃₆O₇

There total 15 articles about C₃₀H₃₆O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 942068-54-4
C₂₁H₂₄O₄

: 942068-64-6
C₃₀H₃₆O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: CH₂Cl₂; acetone / 1 h / 0 °C

2.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

3.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

4.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

5.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

6.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

7.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

8.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

8.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

9.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

10.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

11.1: sodium hydride / tetrahydrofuran / 6 h / Heating

12.1: 19.6 mg / diethyl ether; H₂O / 1.5 h

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096

Reference yield:

: C₂₃H₂₈O₄

: 942068-64-6
C₃₀H₃₆O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: 58 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / toluene / 20 - 70 °C

2.1: CH₂Cl₂; acetone / 1 h / 0 °C

3.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

4.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

5.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

6.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

7.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

8.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

9.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

9.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

10.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

11.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

12.1: sodium hydride / tetrahydrofuran / 6 h / Heating

13.1: 19.6 mg / diethyl ether; H₂O / 1.5 h

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096

Reference yield:

: C₂₁H₂₄O₅

: 942068-64-6
C₃₀H₃₆O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

2.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

3.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

4.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

5.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

6.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

7.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

7.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

8.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

9.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

10.1: sodium hydride / tetrahydrofuran / 6 h / Heating

11.1: 19.6 mg / diethyl ether; H₂O / 1.5 h

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096