Diethylenetriamine pentamethylene phosphonic acid

Base Information

• Chemical Name: Diethylenetriamine pentamethylene phosphonic acid
• CAS No.: 15827-60-8
• Deprecated CAS: 67774-91-8,244775-22-2,291513-72-9,1542224-40-7,1542224-40-7,244775-22-2
• Molecular Formula: C9H28N3O15P5
• Molecular Weight: 573.201
• Hs Code.: HOSPHONIC ACID) PRODUCT IDENTIFICATION
• European Community (EC) Number: 239-931-4
• UNII: 0Q75589TM3
• DSSTox Substance ID: DTXSID0027775
• Nikkaji Number: J219.842H
• Wikipedia: DTPMP
• Wikidata: Q3011490
• RXCUI: 1312549
• Mol file: 15827-60-8.mol

Synonyms:diethylenetriaminepenta(methylenephosphonic) acid;diethylenetriaminepenta(methylenephosphonic) acid, ammonium salt;diethylenetriaminepenta(methylenephosphonic) acid, calcium salt;diethylenetriaminepenta(methylenephosphonic) acid, calcium, octasodium (1:1:8) salt;diethylenetriaminepenta(methylenephosphonic) acid, calcium, sodium salt;diethylenetriaminepenta(methylenephosphonic) acid, dicalcium, hexasodium (1:2:6) salt;diethylenetriaminepenta(methylenephosphonic) acid, dicalcium, sodium (1:2:1) salt;diethylenetriaminepenta(methylenephosphonic) acid, sodium salt;diethylenetriaminepenta-(methylenephosphonic acid);DTPMP cpd;DTPMT

Chemical Property of Diethylenetriamine pentamethylene phosphonic acid

Chemical Property:

• Appearance/Colour: amber viscous liquid
• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.628
• Boiling Point: 1003.3 °C at 760 mmHg
• PKA: 0.59±0.10(Predicted)
• Flash Point: 560.6 °C
• PSA: 346.42000
• Density: 1.945 g/cm³
• LogP: -2.43160
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: Aqueous Base (Sparingly), Water
• Water Solubility.: 500g/L at 25℃
• XLogP3: -15.1
• Hydrogen Bond Donor Count: 10
• Hydrogen Bond Acceptor Count: 18
• Rotatable Bond Count: 16
• Exact Mass: 573.02085218
• Heavy Atom Count: 32
• Complexity: 720

Purity/Quality:

98% ^*data from raw suppliers

Diethylenetriaminepenta(methylenephosphonicacid),technicalgrade50% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,C
• Hazard Codes: Xi,C
• Statements: 36/37/38-51/53-41-37/38
• Safety Statements: 26-36-33-28-23-16-9-39

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Other Classes -> Phosphate Compounds
• Canonical SMILES: C(CN(CP(=O)(O)O)CP(=O)(O)O)N(CCN(CP(=O)(O)O)CP(=O)(O)O)CP(=O)(O)O
• Uses: The phosphonate Diethylenetriaminepenta(methylenephosphonic acid) is a wastewater pollutant, and a component of phosphorous-containing nanoparticles and materials, such as in the preparation of chitosan nanoparticles for plutonium pulmonary decorporation. Diethylenetriaminepentakis(methylphosphonic acid) solution is suitable for use in a study to investigate the dynamics and kinetics of sodium sulfate crystallization in the presence of various organophosphonic acids. It may be employed as ligand for the characterization of Ce3+ complexes by luminescence spectroscopy.

Technology Process of Diethylenetriamine pentamethylene phosphonic acid

There total 4 articles about Diethylenetriamine pentamethylene phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 3-azapentane-1,5-diamine (111-40-0,98824-35-2) → diethylenetriamine penta(methylenephosphonic acid) (15827-60-8,244775-22-2,291513-72-9,67774-91-8)

Guidance literature:

With hydrogenchloride; phosphonic Acid; In water; at 115 ℃; for 2h; Large scale;

Reference yield:

N,N',N',N'',N''-hydroxymethyl-(2-aminoethyl)ethane-1,2-diamine (1542224-36-1) → diethylenetriamine penta(methylenephosphonic acid) (15827-60-8,244775-22-2,291513-72-9,67774-91-8)

Guidance literature:

N,N',N',N'',N''-hydroxymethyl-(2-aminoethyl)ethane-1,2-diamine; With phosphorus(III) oxide; trifluoroacetic acid; In acetonitrile; at 35 - 60 ℃; for 0.333333h; Inert atmosphere;

With water; In acetonitrile; at 85 ℃; for 0.25h; pH=5.4; Inert atmosphere;

Reference yield:

diethylenetriaminopentaacetic acid (67-43-6,84932-15-0) → diethylenetriamine penta(methylenephosphonic acid) (15827-60-8,244775-22-2,291513-72-9,67774-91-8)

Guidance literature:

With phosphorus(III) oxide; methanesulfonic acid; at 55 - 90 ℃; for 2h;

upstream raw materials:

formaldehyd

3-azapentane-1,5-diamine

diethylenetriaminopentaacetic acid

N,N',N',N'',N''-hydroxymethyl-(2-aminoethyl)ethane-1,2-diamine

Downstream raw materials:

diethylenetriamine-N,N,N',N,N-pentaacetic acid pentasodium salt

Refernces

• 1、 -. "PROCESS FOR PRODUCING HIGH-PURITY AMINOMETHYLENE PHOSPHONIC ACID". Paragraph 0047-0051. . Retrieved 2017/05/18.
• 2、 -. "METHOD FOR THE SYNTHESIS OF ALPHA-AMINOALKYLENEPHOSPHONIC ACID". Page/Page column 23. . Retrieved 2014/02/15.