5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

Base Information

Chemical Name:5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione
CAS No.:796034-18-9
Molecular Formula:C₃₅H₂₈O₆
Molecular Weight:544.604
Hs Code.:

Synonyms:5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

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Chemical Property of 5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

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Technology Process of 5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

There total 1 articles about 5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 796034-16-7
2-benzyl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxoborolan-2-yl)phenyl]-benzofuran

: 85060-86-2
2,2-dimethyl-5-(p-bromophenacyl)-1,3-dioxane-4,6-dione

: 796034-18-9
5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In dimethyl sulfoxide; at 80 ℃; for 2h;

Reference yield: 62.0%

: 796034-18-9
5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

: 796739-04-3
4-[4'-(2-benzylbenzofuran-3-yl)biphenyl-4-yl]-4-oxobutyric acid

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 70 ℃; for 6h;

Reference yield:

: 796034-18-9
5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione

: 100-39-0
benzyl bromide

: 796034-19-0
5-benzyl-5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]-dioxane-4,6-dione

Guidance literature:: 5-{2-[4'-(2-benzylbenzofuran-3-yl)-biphenyl-4-yl]-2-oxoethyl}-2,2-dimethyl-[1,3]dioxane-4,6-dione; With sodium hydride; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; at 60 ℃; for 4h;