Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion

Base Information

• Chemical Name: Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion
• CAS No.: 75859-38-0
• Molecular Formula: C₁₈H₁₅N₃O₂
• Molecular Weight: 305.336

Synonyms:Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion

Chemical Property of Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion

Chemical Property:

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Technology Process of Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion

There total 1 articles about Phenyl-2,4,6-triazapentacyclo<6.4.3.0.^2,6.0^7,12.0^9,15>pentadeca-10,13-dien-3,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + bicyclo<4.2.2>deca-2,4,6,9-tetraene (15677-13-1) → Phenyl-2,4,6-triazapentacyclo<6.4.3.0.2,6.07,12.09,15>pentadeca-10,13-dien-3,5-dion (75859-38-0)

Guidance literature:

In 1,4-dioxane; at 85 - 90 ℃; for 4h;

Reference yield: 72.0%

Phenyl-2,4,6-triazapentacyclo<6.4.3.0.2,6.07,12.09,15>pentadeca-10,13-dien-3,5-dion (75859-38-0) → 4-Phenyl-2,4,6-triaza-pentacyclo<6.4.3.02,6.07,12.09,15>pentadeca-3,5-dion (75891-06-4)

Guidance literature:

With hydrogen; platinum on activated charcoal; In ethyl acetate; for 3h;

Reference yield:

Phenyl-2,4,6-triazapentacyclo<6.4.3.0.2,6.07,12.09,15>pentadeca-10,13-dien-3,5-dion (75859-38-0) → 7,8-Diazatetracyclo<4.3.3.02,10.05,9>dodecan-7-carbonsaeure-N-phenylamid (75891-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / H₂ / Pt/C (5percent) / ethyl acetate / 3 h

2: 1.) KOH, H₂O/DMSO, 2.) NH₄Cl aq. / 1.) 1 h room temperature, 2.) 0 deg C

With potassium hydroxide; water; hydrogen; ammonium chloride; dimethyl sulfoxide; platinum on activated charcoal; In ethyl acetate;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

bicyclo<4.2.2>deca-2,4,6,9-tetraene

Downstream raw materials:

7,8-Diazatetracyclo<4.3.3.0^2,10.0^5,9>dodeca-3,11-dien-8-carbonsaeure-N-phenylamid

7,8-Diazatetracyclo<4.3.3.0^2,10.0^5,9>dodeca-3,11-dien-7-carbonsaeure-N-phenylamid

4-Phenyl-2,4,6-triaza-pentacyclo<6.4.3.0^2,6.0^7,12.0^9,15>pentadeca-3,5-dion

7,8-Diazatetracyclo<4.3.3.0^2,10.0^5,9>dodecan-7-carbonsaeure-N-phenylamid

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