methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

Base Information

Chemical Name:methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose
CAS No.:1092935-53-9
Molecular Formula:C₂₂H₂₅N₃O₆
Molecular Weight:427.457
Hs Code.:

Synonyms:methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

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Chemical Property of methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

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Technology Process of methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

There total 1 articles about methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1092935-52-8
methyl 2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

: 100-39-0
benzyl bromide

: 1092935-53-9
methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

Guidance literature:: methyl 2-azido-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 20 ℃;
DOI:10.1016/j.carres.2008.06.011

Reference yield: 43.0%

: 1092935-53-9
methyl 2-azido-3-O-benzyl-2-deoxy-4,6-O-(4-methoxybenzylidene)-α/β-D-glucopyranose

: 1092935-54-0
methyl 2-azido-3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: 501088-18-2
methyl 2-azido-3-O-benzyl-2-deoxy-6-O-(4-methoxybenzyl)-α-D-glucopyranoside

Guidance literature:: With sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2008.06.011