α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

Base Information

Chemical Name:α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid
CAS No.:85208-14-6
Molecular Formula:C₁₈H₂₁N₃O₆S
Molecular Weight:407.447
Hs Code.:

Synonyms:α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

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Chemical Property of α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

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Technology Process of α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

There total 6 articles about α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92592-16-0
ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

: 85208-14-6
α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

Guidance literature:: With potassium hydroxide; In ethanol; for 1.5h; Yield given; Ambient temperature;
DOI:10.1021/jm00092a006

Reference yield:

: 60845-81-0
ethyl 2-amino-α-(hydroxyimino)-4-thiazole acetate

: 85208-14-6
α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, HCl / 10percent Pd/C / ethanol

2: aq. K₂CO₃ / tetrahydrofuran / 24 h / Ambient temperature

3: aq. sodium bicarbonate / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

4: aq. KOH / ethanol / 1.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; hydrogen; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00092a006

Reference yield:

: 60846-29-9
ethyl 2-amino-α-(N-(t-butoxycarbonyl)amino)-4-thiazoleacetate

: 85208-14-6
α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. sodium bicarbonate / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

2: aq. KOH / ethanol / 1.5 h / Ambient temperature

With potassium hydroxide; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00092a006