3-Iodo-2-methylbenzotrifluoride

Base Information

• Chemical Name: 3-Iodo-2-methylbenzotrifluoride
• CAS No.: 863111-55-1
• Molecular Formula: C₈H₆F₃I
• Molecular Weight: 286.035
• Mol file: 863111-55-1.mol

Synonyms:1-iodo-2-methyl-3-(trifluoromethyl)benzene

Chemical Property of 3-Iodo-2-methylbenzotrifluoride

Chemical Property:

Purity/Quality:

3-Iodo-2-methylbenzotrifluoride 97% ^*data from reagent suppliers

Safty Information:

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Technology Process of 3-Iodo-2-methylbenzotrifluoride

There total 1 articles about 3-Iodo-2-methylbenzotrifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-methyl-3-trifluoromethylaniline (54396-44-0) → 1-iodo-2-methyl-3-(trifluoromethyl)benzene (863111-55-1)

Guidance literature:

2-methyl-3-trifluoromethylaniline; With sulfuric acid; sodium nitrite; In water; at 0 ℃;

With potassium iodide; In water; at 0 - 20 ℃;

DOI:10.1021/ol802185x

Reference yield: 88.0%

1-iodo-2-methyl-3-(trifluoromethyl)benzene (863111-55-1) + 2-(Trimethylsilyl)ethanol (2916-68-9) → trimethyl[2-(2-methyl-3-trifluoromethylphenoxy)ethyl]silane (1338215-42-1)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In toluene; at 110 ℃; for 14h; Inert atmosphere; Sealed tube;

DOI:10.1016/j.tetlet.2011.08.023

Reference yield: 82.0%

1-iodo-2-methyl-3-(trifluoromethyl)benzene (863111-55-1) + bis(pinacol)diborane (73183-34-3) → 2,2'-(4-methyl-5-(trifluoromethyl)-1,3-phenylene)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:

at 15 ℃; for 14h; Time; regioselective reaction; UV-irradiation; Photolysis;

DOI:10.1021/jacs.6b05436

upstream raw materials:

2-methyl-3-trifluoromethylaniline

Downstream raw materials:

4-benzyl-2-methyl-1-(trifluoromethyl)benzene

C₁₆H₁₂F₃N

2-methyl-3-trifluoromethylphenol

trimethyl[2-(2-methyl-3-trifluoromethylphenoxy)ethyl]silane

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