Technology Process of (1S,2R)-1-phenyl-2-methyl-2,3-epoxypropyl alcohol
There total 5 articles about (1S,2R)-1-phenyl-2-methyl-2,3-epoxypropyl alcohol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
vinyl acetate;
In
various solvent(s);
at 30 ℃;
for 24h;
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
lipase PS (Amano);
DOI:10.3987/COM-94-S97
- Guidance literature:
-
Multi-step reaction with 3 steps
1: MCPBA / CHCl3 / 10 h / Ambient temperature
2: various solvent(s) / 17 h / 30 °C / lipase PS (Amano)
3: 10percent aq. NaOH / methanol / 2 h
With
sodium hydroxide; 3-chloro-benzenecarboperoxoic acid;
In
methanol; chloroform;
DOI:10.3987/COM-94-S97
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 68 percent / H2O / 63 h / 28 °C / baker's yeast
2: MCPBA / CHCl3 / 10 h / Ambient temperature
3: various solvent(s) / 17 h / 30 °C / lipase PS (Amano)
4: 10percent aq. NaOH / methanol / 2 h
With
sodium hydroxide; 3-chloro-benzenecarboperoxoic acid;
In
methanol; chloroform; water;
DOI:10.3987/COM-94-S97
