C₂₆H₄₀O₄Si

Base Information

Chemical Name:C₂₆H₄₀O₄Si
CAS No.:1431725-63-1
Molecular Formula:C₂₆H₄₀O₄Si
Molecular Weight:444.687
Hs Code.:

C<sub>26</sub>H<sub>40</sub>O<sub>4</sub>Si

Synonyms:C₂₆H₄₀O₄Si

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Chemical Property of C₂₆H₄₀O₄Si

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Technology Process of C₂₆H₄₀O₄Si

There total 1 articles about C₂₆H₄₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₆H₃₈O₂Si

: 1431725-63-1
C₂₆H₄₀O₄Si

Guidance literature:: With methanesulfonamide; AD-mix-α; water; In tert-butyl alcohol; at 0 ℃; for 48h;
DOI:10.1002/anie.201203406

Reference yield: 78.0%

: 1431725-63-1
C₂₆H₄₀O₄Si

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1431725-64-2
C₃₈H₆₈O₄Si₃

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201203406

Reference yield:

: 1431725-63-1
C₂₆H₄₀O₄Si

: 1431725-77-7
C₄₉H₈₆O₁₂Si₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

2.1: thionyl chloride; pyridine / dichloromethane / 0.05 h / 0 °C

3.1: H₃N*FH*3H₂O / methanol / 12 h / Inert atmosphere; Reflux

4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 0 °C / Inert atmosphere

5.2: 1 h / -78 °C / Inert atmosphere

6.1: dipyridine chromium trioxide / dichloromethane / 0 - 20 °C

7.1: samarium diiodide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

8.1: ammonium fluoride-hydrogen fluoride / methanol / 48 h / Inert atmosphere; Reflux

9.1: 2,6-dimethylpyridine / dichloromethane / -78 - 0 °C / Inert atmosphere

10.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / -78 - 20 °C / Inert atmosphere

10.2: Inert atmosphere

11.1: water; methanesulfonamide; AD-mix-β / tert-butyl alcohol / 48 h / 0 °C

12.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / Inert atmosphere

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; n-butyllithium; thionyl chloride; samarium diiodide; ammonium fluoride-hydrogen fluoride; methanesulfonamide; AD-mix-β; H₃N*FH*3H₂O; water; dipyridine chromium trioxide; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 10.2: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201203406