chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

Base Information

Chemical Name:chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin
CAS No.:99643-58-0
Molecular Formula:C₃₀H₂₇ClSn
Molecular Weight:541.707
Hs Code.:

Synonyms:chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

Chemical Property:

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Technology Process of chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

There total 4 articles about chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 753-73-1
dimethyltin dichloride

: 20195-60-2
1,1-dimethyl-2,3,4,5-tetraphenylstannole

: 99643-58-0
chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

Guidance literature:: With ethanol; In ethanol; dichloromethane; water; under N2 or Ar, Ph4C4SnMe2, Me2SnCl2, 95% EtOH, and CH2Cl2 heated at reflux for 15 min; evapd., crystals pptd.;
DOI:10.1021/ja00263a006

Reference yield: 34.0%

: 753-73-1
dimethyltin dichloride

: 21289-08-7,99643-57-9
(E,E)-(1,2,3,4-tetramethyl-1,3-butadien-1,4-ylidene)-dilithium

: 99643-58-0
(1,2,3,4-tetraphenylbuta-1,3-dienyl)dimethyltin chloride

Guidance literature:: With water; In tetrahydrofuran; inert atmosphere; addn. of Li-compd. to Sn-compd., stirring at room temp. overnight, hydrolytic extn.; chromy. (SiO2), recrystn. (i-PrOH);
DOI:10.1021/ic980662d

Reference yield:

: 21289-08-7,99643-57-9
(E,E)-(1,2,3,4-tetramethyl-1,3-butadien-1,4-ylidene)-dilithium

: 99643-58-0
chlorodimethyl(E,E)-(1,2,3,4-tetraphenyl-1,3-butadien-1-yl)tin

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran

2: ethanol / dichloromethane; water; ethanol

With ethanol; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1021/ja00263a006