3-(2,3-Dimethylphenyl)propanoic acid

Base Information

Chemical Name:3-(2,3-Dimethylphenyl)propanoic acid
CAS No.:25173-73-3
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:
DSSTox Substance ID:DTXSID601299935

Synonyms:3-(2,3-dimethylphenyl)propanoic acid;25173-73-3;dimethylbenzenepropanoic acid;SCHEMBL1450886;2,3-Dimethylbenzenepropanoic acid;DTXSID601299935;3-(2,3-dimethylphenyl)propanoicacid;AKOS005217146;CS-0345905;EN300-1843585

Suppliers and Price of 3-(2,3-Dimethylphenyl)propanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 3-(2,3-Dimethylphenyl)propanoic acid

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:178.099379685
Heavy Atom Count:13
Complexity:177

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)CCC(=O)O)C

Technology Process of 3-(2,3-Dimethylphenyl)propanoic acid

There total 8 articles about 3-(2,3-Dimethylphenyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5779-93-1
2,3-dimethylbenzaldehyde

: 25173-73-3
3-(2,3-Dimethylphenyl)-propansaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 90.7 percent / pyridine, piperidine / 48 h / 80 °C

2: 95.8 percent / H₂ / 10percent Pd/C / dioxane / 517.1 - 1551.4 Torr

With piperidine; pyridine; hydrogen; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1007/BF00807400

Reference yield:

: 87-59-2
2,3-Dimethylaniline

: 25173-73-3
3-(2,3-Dimethylphenyl)-propansaeure

Guidance literature:: Multi-step reaction with 6 steps

1: 40 percent / HBr / diazotization

2: 1.) Mg / 1.) ether, 2.) ether, reflux, 2 h; room temp., overnight

3: 98.5 percent / LiAlH₄ / diethyl ether / 1.) reflux, 3 h, 2.) room temp., overnight

4: 80.1 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

5: 90.7 percent / pyridine, piperidine / 48 h / 80 °C

6: 95.8 percent / H₂ / 10percent Pd/C / dioxane / 517.1 - 1551.4 Torr

With piperidine; pyridine; lithium aluminium tetrahydride; hydrogen bromide; hydrogen; magnesium; pyridinium chlorochromate; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1007/BF00807400

Reference yield:

: 13651-14-4
(2,3-dimethylphenyl)methanol

: 25173-73-3
3-(2,3-Dimethylphenyl)-propansaeure

Guidance literature:: Multi-step reaction with 3 steps

1: 80.1 percent / PCC / CH₂Cl₂ / 2 h / Ambient temperature

2: 90.7 percent / pyridine, piperidine / 48 h / 80 °C

3: 95.8 percent / H₂ / 10percent Pd/C / dioxane / 517.1 - 1551.4 Torr

With piperidine; pyridine; hydrogen; pyridinium chlorochromate; palladium on activated charcoal; In 1,4-dioxane; dichloromethane;
DOI:10.1007/BF00807400