Technology Process of C19H19N5O2
There total 4 articles about C19H19N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine hydrate / methanol / Reflux
2: sulfuric acid / 80 °C
3: triphenylphosphine; caesium carbonate / palladium diacetate / dimethyl sulfoxide / 2 h / 100 °C / Inert atmosphere
With
sulfuric acid; caesium carbonate; hydrazine hydrate; triphenylphosphine;
palladium diacetate;
In
methanol; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: titanium(III) chloride / tetrahydrofuran / 48 h / 20 °C
3: triphenylphosphine; caesium carbonate / palladium diacetate / dimethyl sulfoxide / 2 h / 100 °C / Inert atmosphere
With
titanium(III) chloride; potassium carbonate; caesium carbonate; triphenylphosphine;
palladium diacetate;
In
tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: titanium(III) chloride / tetrahydrofuran / 48 h / 20 °C
2: triphenylphosphine; caesium carbonate / palladium diacetate / dimethyl sulfoxide / 2 h / 100 °C / Inert atmosphere
With
titanium(III) chloride; caesium carbonate; triphenylphosphine;
palladium diacetate;
In
tetrahydrofuran; dimethyl sulfoxide;