benzyl 6β-penicillanate

Base Information

Chemical Name:benzyl 6β-penicillanate
CAS No.:75636-71-4
Molecular Formula:C₁₉H₂₁Cl₆N₂O₆PS
Molecular Weight:649.143
Hs Code.:

benzyl 6β-<bis-(2,2,2-trichloroethyl)phosphoramido>penicillanate

Synonyms:benzyl 6β-penicillanate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 6β-penicillanate

Chemical Property:

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Technology Process of benzyl 6β-penicillanate

There total 1 articles about benzyl 6β-penicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 17672-53-6
bis-(2,2,2-trichloroethyl)phosphorochloridate

: 3956-31-8,49626-54-2,64519-71-7
(2S,6R)-6-Amino-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzyl ester

: 75636-71-4
benzyl 6β-penicillanate

Guidance literature:: With pyridine; In dichloromethane; for 2h; Ambient temperature;

Reference yield: 76.0%

: 865-34-9
lithium methanolate

: 75636-71-4
benzyl 6β-penicillanate

: 62801-95-0
(2S,6S)-6-[Bis-(2,2,2-trichloro-ethoxy)-phosphorylamino]-6-methoxy-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid benzyl ester

Guidance literature:: With tert-butylhypochlorite; In tetrahydrofuran; methanol; at -78 ℃; for 0.5h;

Reference yield:

: 75636-71-4
benzyl 6β-penicillanate

: 35353-33-4,35353-37-8,72888-72-3
benzyl 6α-methoxy-6β-(phenylacetamido)penicillanate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / t-butyl hypochlorite / tetrahydrofuran; methanol / 0.5 h / -78 °C

2: 45 percent / triethylamine, 9percent n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

With n-butyllithium; tert-butylhypochlorite; triethylamine; In tetrahydrofuran; methanol; hexane;