2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

Base Information

Chemical Name:2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one
CAS No.:844879-61-4
Molecular Formula:C₂₄H₁₉F₂N₃O₂
Molecular Weight:419.431
Hs Code.:

Synonyms:2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

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Chemical Property of 2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

Chemical Property:

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Technology Process of 2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

There total 1 articles about 2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.2%

: 844879-60-3
2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl) ethanone

: 74-88-4
methyl iodide

: 844879-61-4
2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

Guidance literature:: 2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl) ethanone; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 1h;

methyl iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2.5h;

Reference yield:

: 844879-61-4
2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one

: trimethylsulfoxonium iodide

: 844879-62-5
3-(4-benzyloxy-phenyl)-1-{1-[2-(2,4-difluoro-phenyl)-oxiranyl]-ethyl}-1H-[1,2,4]triazole

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 1h;

2-[3-(4-benzyloxyphenyl)-1,2,4-triazol-1-yl]-1-(2,4-difluorophenyl)propan-1-one; In dimethyl sulfoxide; at 20 ℃; for 3h;